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  • 1
    ISSN: 0887-624X
    Keywords: monodisperse particles ; emulsion copolymerization, divinylbenzene ; porous particles ; macroporous structure ; linear polymer, diluent ; crosslinked domains ; Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Notes: Monodisperse porous polymer particles in the size range of 10 μm in diameter were prepared via seeded emulsion polymerization. Linear polymer (polystyrene seed) or a mixture of linear polymer and solvent or nonsolvent were used as inert diluents. The pore diameters of these porous polymer particles were on the order of 1000 Å with pore volumes up to 0.9 mL/g and specific surface areas up to 200 m2/g. The physical features of the porous polymer particles depended on the diluent type and the crosslinker content, as well as the molecular weight of polymer seed particles. By varying the molecular weight of the linear polymer, monodisperse porous polymer particles with different pore size distribution could be synthesized. Polymer seed with a low degree of crosslinking instead of linear polymer could also be used to prepare monodisperse porous polymer particles with smaller pore volume and pore size.
    Additional Material: 11 Ill.
    Type of Medium: Electronic Resource
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  • 2
    Electronic Resource
    Electronic Resource
    [S.l.] : American Institute of Physics (AIP)
    Review of Scientific Instruments 57 (1986), S. 2332-2338 
    ISSN: 1089-7623
    Source: AIP Digital Archive
    Topics: Physics , Electrical Engineering, Measurement and Control Technology
    Notes: A stainless-steel piston cylinder dilatometer (volume ∼100 cm3), designed for use in microgravity, was tested and modified for the purpose of obtaining the polymerization kinetics of monodisperse polystyrene latexes, as well as the latexes themselves. A low-speed, oscillatory agitation (10 rpm, 30° arc per cycle) and redesigned stir paddle were selected for the low shear requirements of the microgravity experiments. Conversion histories accurate to within 2% were obtained after apparatus modification and procedural changes were implemented.
    Type of Medium: Electronic Resource
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