Complete separation of bile acids in serum from cholesterol
Analysis time less than 15 min, adaptable to GC/MS
Analytical Chemistry and Spectroscopy
Wiley InterScience Backfile Collection 1832-2000
Chemistry and Pharmacology
The proposed combination of a rather simple procedure for sample preparation with capillary gas-liquid chromatography using a barium carbonate/polyethyleneglycol 20,000 column and a Grob-type on-column injector permits measurement of bile acids in serum with high separation efficiency, short analysis time and complete separation of bile acids from cholesterol. The method can be adapted to combined capillary gas-liquid chromatography - mass spectrometry.
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