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  • 1
    ISSN: 0044-2313
    Keywords: Chemistry ; Inorganic Chemistry
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Description / Table of Contents: This paper contains: 1The synthesis of the 1.3-disilacyclopentenes (a)(b)(2) and of the 1.3-disilacyclo-butane (c); formulas see above.2The synthesis of the 1.3-disilacyclopentane skeleton (d) and of the SiCl-functional derivatives (e) (f ) (g) (h) (i) as well as of SiH-containing derivatives, e.g. (j).3The chlorination of (i) with SO2,Cl2, yielding (k) and (l), and the formation of (m) from (k) with K-methypyrrolidine.4The synthesis of the spirane (n).5The synthesis of the ten-membered ring(o) and of the unsaturated derivatives (p)and (q). Besides the synthetic routes, spectroscopic data (ir, pmr, and mass spectra) of the cyclic compounds as well as of the intermediate products are given.
    Notes: Es wird berichtet über: 1Die Synthese der 1,3-disilacyclopentene (a) (b)2 und des 1,3-disila-cyclobutans (c) 2Die Synthese des 1,3-Disilacyclopentan-Gerüstes (d) und der SiCl-funktionellen Derivate (e)(f)(g)(h)(i)sowie der SiH haltigen Derivate, z. B. (j) 3Die Chlorierung von (i) mit SO2Cl2 zu (k) und (1) und die Bildung ron (m) aus (k) mit K-Methylpyrrolidin 4Die Synthese des Spirans (n) 5Die Synthese des 10-Ringes (o) und der nngesattigten Derivate (p) und (q). SeFen den Synthesewegen werden spelitroskopische Daten und PMR-Spektren der cyclischen Verhindungen sou ie der Zwischenprodukte angegeben.
    Additional Material: 6 Ill.
    Type of Medium: Electronic Resource
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