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  • 1
    Electronic Resource
    Electronic Resource
    Weinheim : Wiley-Blackwell
    Zeitschrift für anorganische Chemie 620 (1994), S. 519-522 
    ISSN: 0044-2313
    Keywords: Zirconium complexes ; diazabutadiene ligands ; Chemistry ; Inorganic Chemistry
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Description / Table of Contents: Zirconium Diazabutadiene Complexes of the Type Zr(DAD)31,4-Diazabutadienes (DAD), RN=CPh—CPh=NR 1 (R = C6H5 a, CH3C6H4 b, CH3OC6H4 c), react with ZrCl4 · 2 THF with formation of complexes of the type ZrCl4 · DAD 2. At interaction with lithium diazadienides Li2DAD deep coloured complexes of the composition Zr(DAD)3 3 are formed.The new compounds were characterized by elemental analysis, i.r., 1H- and 13C-n.m.r. spectra.
    Notes: 1,4-Diazabutadiene (DAD), RN=CPh—CPh=NR 1 (R=C6H5 a, CH3C6H4 b, CH3OC6H4 c), reagieren mit ZrCl4 · 2 THF zu Addukten der Zusammensetzung ZrCl4 · DAD 2. Diese werden bei Einwirkung von Lithiumdiazadieniden Li2DAD in tieffarbige Komplexe des Typs Zr(DAD)3 3 übergeführt.Die erhaltenen Verbindungen wurden durch Elementaranalysen sowie ihre IR-, 1H- und 13C-NMR-Spektren charakterisiert.
    Additional Material: 2 Ill.
    Type of Medium: Electronic Resource
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